Version 1.0Melting PointApparatus SMP40Instructions for useautomatic melting pointSMP40Dynalab Corp. 350 Commerce Drive Rochester, NY 14623Tel: 585-3
1 Selecting an Alphanumeric Entry Field opens the text keypad interface.2 The alphanumeric entry field can be populated with letters (Abc), numbers
1 Selecting a Date Entry Field opens the date keypad interface.2 The date entry field is displayed in the format specified in the User Settings menu
105.2.6 Drop Down List Field1 Selecting a Drop Down List Field displays the options available for that field.2 Arrows keys may be displayed to in
116.1 Creating a New MethodIn the Measurement menu screen touch the “Create a new measurement” section of the screen.1 Enter a sample name for the
6.2 Preset MethodsIn the Measurement menu screen touch the “Use a preset from the library” section of the screen.121 In the preset methods screen se
8 The option of saving this new method as a new preset method will be given if the sample name has been changed. Select “Yes” to save the method for
7. Performing Melt DeterminationsOnce the analysis method and sample information have been entered into the SMP40 software the instrument will display
153 The instrument status will change to “Heating” and the command toolbar options will change.4 The SMP40 will quickly heat the sample block to the
168 As the melt determination progresses the capillary tube melt status changes through:Solid: No changes have been detected in the samples physical
178. ResultsTouching the results section on the main menu screen will open the results menu. Two options are now available:View previous results: Dis
1. Introduction 12. Safety Advice Before Use 13. General Description 1 3.1 Module Separation 2 3.2 Melting Point Determination 3 3.3
18Rename: The Rename action is used to change the Sample Name for the selected result.Delete: The Delete action is used to delete the selected result
194 The required option should be selected from the displayed list or alternatively enter the search criteria using the keypad that is displayed.5 W
208.1.2 Opening Results FilesWhen a melt determination is complete or a result file is opened, the screen will display the Report Screen.The report
218.1.3 Viewing VideosWhen a video record is accessed the Video Replay screen is displayed.Block temperature at specific timeSelected capillaryVideo r
221 To start the video replay press the play button () in the video replay controls. Once the play button has been pressed it will change to a pause
231 Select the capillary tube to which the manual event is to be added by pressing the relevant “Capillary selection” button.2 Select the timeframe
24The melt determination report is updated with any manual events that are added and saved. An asterisk next to the event name is used to denote that
258.1.5 Deleting Result Files8.2 Re-use Result Parameters1 To delete individual results from the instruments memory highlight the result to be delet
269 File ManagementTouching the File Management section on the main menu screen will open the File Management menu. Two options are now available:Mana
9.1.1 Select All/Clear Selection1 Pressing the “Select All” button in the Manage Files toolbar will highlight all of the result files.2 If
1. IntroductionThank you for purchasing this piece of Stuart equipment. To get the best performance from the SMP40 please read these instructions care
3 Once the move action has been completed the files will no longer be available on the instrument so ensure that no further reprocessing of the resul
10 Settings and CalibrationTouching the Settings and Calibration section on the main menu screen will open the Settings and Calibration menu. There ar
Set time: The devices displayed time can be set using the time keypad interface.Set date: The devices displayed date can be set using the date keypad
10.2 Maintenance SettingsIn the Settings and Calibration menu screen touch the Change maintenance settings section of the screen. The Maintenance scr
For information on where to purchase suitable certified reference materials please contact us: [email protected]: +44 (0)1785 810433I
10.3.1 Current Calibration FactorThe current calibration factor shows the factor which is used to calculate the displayed block temperature on the dev
8 In the Select Calibration screen highlight the result file to be used for the first calibration point.9 Press the "Select result and continue
15 The calibration screen is now updated to show the new calibration details. The Calibration history window will now update to display details of th
11. Maintenance & ServicingWARNING: Ensure the unit is disconnected from the mains electricity supply before attempting maintenance or servicin
12. WarrantyStuart warrants this instrument (excluding the VGA touch screen) to be free from defects in material and workmanship when used under norma
3.1 Module SeparationFigure 1: SMP40 module separationThe SMP40 can be split into two separate modules using the split module release mechanism locate
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This product meets the applicable EC harmonized standards for radio frequency interference and may be expected not to interfere with, o
INSPECTION REPORT MODEL SMP40 ELECTRICAL SAFETY 1. Earth continuity 2. Insulation 3. Flash test FUNCTIONAL 1. Indicator
3.2 Melting Point DeterminationThe capillary technique is a standard method for determining the melting point of a substance. In this method, thin gla
The SMP40 can accommodate up to three sample capillaries. For accurate melting point determinations it is recommended that three samples of the same m
5. Instrument and Software Controls5.1 Instrument Mains On/Off: This is a rocker type switch found on the left hand side o
When the instrument is first switched on the display will show “LOADING PLEASE WAIT” message. After 30 seconds the display will show the main menu scr
The command toolbar is located at the bottom of the screen in most menus within the software interface. The command toolbar will give the user either
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